S. S. Hossain, J. W. Bullard | 2026 | Materials Letters
DOI 10.1016/j.matlet.2026.140312Review state
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This paper presents a method for shaping and sintering synthetic lunar regolith to create structural components. The process involves freeze-drying and sintering the regolith at high temperatures, followed by infiltration with a binding agent to enhance mechanical properties. The results show that the sintered regolith can achieve high compressive strength and maintain structural integrity under various conditions. The study highlights the potential of using lunar regolith as a construction material for future lunar missions. This paper describes the fabrication of complex near-net shapes from synthetic lunar regolith using freeze casting and sol infiltration. The process involves sintering at 1000°C and 1100°C, and infiltration with sodium silicate solution to achieve relative densities of 80% and compressive strengths up to 1200 MPa. The method is suitable for lunar polar regions due to natural freezing and sublimation conditions. This paper describes a hybrid process for manufacturing near-net shape parts from synthetic lunar regolith using freeze-casting, sublimation, sintering, and sol infiltration. The synthetic regolith (OPRH2N) is combined with sodium metasilicate solutions
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Freeze casting in Na2SiO3 sol
Fabrication | Lunar construction
SEM analysis of fracture surfaces
Microstructural analysis | Lunar construction
Infiltration with sodium silicate solution
Material infiltration | Lunar construction
Compatibility with lunar polar regions
Environmental analysis | Lunar construction
freeze-casting
shaping
sintering
processing
infiltration
processing
capillary pressure measurement
characterization
Infiltration solution
30 wt% sodium silicate solution
Freeze casting
Na2SiO3 sol
Compatibility with lunar polar regions
Cold and vacuum enable natural freezing and sublimation
relative density
38% to 43%
compressive strength
3.5 MPa
compressive strength
60 MPa
sintering temperature
1000 C to 1150 C
infiltration cycles
1 to 3